江汉大学学报(自然科学版) ›› 2020, Vol. 48 ›› Issue (1): 29-36.doi: 10.16389/j.cnki.cn42-1737/n.2020.01.004

• 化学 • 上一篇    下一篇

山楂中黄酮类物质的水提取工艺及理化性质研究

郭艳华,李娇,黄刚,吴旺喜,白建勋,张彩红,熊加严   

  1. 江汉大学 化学与环境工程学院,湖北 武汉 430056
  • 发布日期:2020-01-20
  • 作者简介:郭艳华(1960— ),女,教授,研究方向:天然产物化学及功能材料。
  • 基金资助:
    湖北省教育厅科技项目(B2014073)

Study on Water Extraction Process and Physicochemical Properties of Flavonoids in Hawthorn

GUO Yanhua,LI Jiao,HUANG Gang,WU Wangxi,BAI Jianxun,ZHANG Caihong,XIONG Jiayan   

  1. School of Chemical and Environmental Engineering,Jianghan University,Wuhan 430056,Hubei,China
  • Published:2020-01-20

摘要: 探讨水提取山楂中黄酮的工艺条件,考察浸提时间、温度、料液比、酸度等条件对提取山楂中总黄酮含量的影响;用化学显色反应和紫外光谱初步确定提取产物的黄酮类型;研究山楂黄酮的理化性质。结果表明:水提取山楂黄酮的适宜工艺条件为:提取时间2 h,温度50 ℃,山楂与蒸馏水的料液比为1∶30,酸度pH = 8,黄酮得率为4. 96%。经显色反应和紫外光谱初步确定山楂黄酮的类型为黄酮醇类和简单黄酮类。食品添加剂和金属离子对山楂黄酮含量及抗氧化活性均有一定的影响。

关键词: 山楂, 水提取工艺, 黄酮含量, 紫外光谱, 理化性质, 抗氧化活性

Abstract: The process conditions of flavonoids extracted from hawthorn with water were discussed. The effects of extraction time,temperature,solid-liquid ratio and acidity on flavonoids extracted from hawthorn were investigated;the extracted flavonoids type was determined by chemical color reaction and UV spectroscopy;the physical and chemical properties were investigated. The results showed that the suitable process conditions of water extraction of hawthorn flavone were as follows:the extracting time of 2 h,the temperature of 50 ℃ ,the solid-liquid ratio of hawthorn with distilled water of 1∶30,the acidity of pH = 8,the yield of flavonoids was 4. 96% under these conditions. The types of flavonoids from hawthorn which determined by color reaction and UV spectrum were flavonols and simple flavonoids. Food additives and metal ions had certain influence on the flavonoids content and the antioxidant activity of flavonoids.

Key words: hawthorn, water extraction process, flavonoid content, ultraviolet spectrum, physicochemical properties, antioxidant activity

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